Answer:
Explanation:
[tex]\text{The steps shown below indicate the rearrangement of the experiment.}[/tex]
[tex]\text{e. Add the crude reaction mixture to the separatory funnel}[/tex]
[tex]\text{f. Extract chloroaniIic acid by adding 5\%. HCl solution to the crude reaction mixture }[/tex]
[tex]\text{l. Mix/vent then drain off the aqueous layer}[/tex]
[tex]\text{i. Extract benzociane by adding 5\% NaOH solution to the organic layer}[/tex]
[tex]\text{c. Mix/vent then drain off the organic layer}[/tex]
[tex]\text{d. Add sodium sulfate to the aqueous layer to remove aw residual water}[/tex]
[tex]\text{a. Drain off the remaining organic from the tip of the separatory funnel}[/tex]
[tex]\text{h. Decant the into a round bottom flask and use the rotavap to evaporate solvent}[/tex]
[tex]\text{b. Weight out the product and determine Its MP}[/tex]